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NMR Concepts & Operating Techniques 06

Spectrometer Set-Up and Calibration

   Watch Promo

Dr. Traficante describes the calibration techniques used for quality-testing NMR spectrometers, especially measuring sensitivity and the 9O-degree pulse width. A trouble-shooting chart is presented and shown how to use it to help identify the source of the problem if these or other parameters do not meet specifications.

  • Impedance Matching
  • Ringing
  • Shimming
  • Measuring the 90-degree Pulse
  • Trouble-Shooting Chart


Your Instructor


Daniel D. Traficante
Daniel D. Traficante

Dr. Traficante obtained his Ph.D. in 1962 from MIT in the field of synthetic organic chemistry. He has worked in the NMR field since 1962, and in the early 1970s he pioneered multi-nuclear instrumentation. He has built probes, reassembled spectrometers, and developed new software programs to enhance the signal-to-noise ratio and the resolution of NMR spectra. His current research in the areas of structure determination, instrumentation, and data processing provide him with knowledge and expertise that are applicable to a broad audience. His organic chemistry background, plus his expertise in electronics, gives his lectures a special depth and appreciation for the field. Dr. Traficante is known throughout the world as an outstanding educator.


Class Curriculum


  Basic Concepts In NMR
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